Progress of Chromatography-Mass Spectrometry Technology and Development of Pesticide Multi-residue Analysis Methods (Part 2)——On the Selectivity of Low Resolution Mass Spectrometry

LI Chong-jiu

doi:10.7538/zpxb.2021.0143

Journal of Chinese Mass Spectrometry Society > 2021 > 42(5): 681-690. > DOI: 10.7538/zpxb.2021.0143 CSTR: 32365.14.zpxb.2021.0143

LI Chong-jiu. Progress of Chromatography-Mass Spectrometry Technology and Development of Pesticide Multi-residue Analysis Methods (Part 2)——On the Selectivity of Low Resolution Mass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2021, 42(5): 681-690. DOI: 10.7538/zpxb.2021.0143

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Progress of Chromatography-Mass Spectrometry Technology and Development of Pesticide Multi-residue Analysis Methods (Part 2)——On the Selectivity of Low Resolution Mass Spectrometry

LI Chong-jiu

China Agricultural University, Beijing 100091, China

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Abstract

This paper reviewed the development of chromatography-mass spectrometry about promoting the analysis of multi-pesticide residues from the selectivity of low resolution mass spectrometry. The progress of mass spectrometry technology had changed the analytical method of pesticide residues. On the basis of clarifying the molecular structure of sample disruptors, the corresponding sample pretreatment method was established. The selective detector of chromatography was replaced by mass spectrometry detector which collected molecular structure information. Selective ion detection technology and tandem mass spectrometry technology improved the ability of eliminate interferents. Based on mass spectrometry, methods for simultaneous multi-residue analysis of multiple pesticides were established.
- chromatography-mass spectrometry,
- low resolution mass spectrometry,
- pesticide residue

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[1]	蔡盛林. 中国农业百科全书：农药卷[M]. 北京：农业出版社，1993.
[2]	ZWEIG G. Analytical methods for pesticides, plant growth reglulators, and food additives[M]. Academic Press, 1963.
[3]	唐英章. 现代食品安全检测技术[M]. 北京：科学出版社，2004.
[4]	NY/T 761—2008蔬菜和水果中有机磷、有机氯、拟除虫菊酯和氨基甲酸酯类农药多残留的测定[S]. 北京：农业出版社，2008.
[5]	农药残留分析质量控制程序——欧盟农药残留监测指南[R]. 中国标准化, 2003: 46-56.
[6]	COOK J, ENGEL M, WYLIE P, QUIMBY B. Multiresidue screening of pesticides in foods using retention time locking, GC-AED, database search, and GC/MS identification[J]. Journal of AOAC International, 1999, 82(2): 313-326.
[7]	农药残留影响及其测定方法[M]. 陈筱侠译. 上海：上海科学技术文献出版社，1980: 35-45.
[8]	王维国，李重九，李玉兰，徐建忠. 有机质谱应用[J]. 北京：化学工业出版社，2006.
[9]	樊德方. 农药残留量分析与检测[M]. 上海：上海科学技术出版社，1982.
[10]	宋淑玲，李重九，马晓东. 蔬菜农药多残留分析中基质共提物净化方法的研究[J]. 分析测试学报，2008,27(8):795-799. SONG Shuling, LI Chongjiu, MA Xiaodong. Study on cleanup method for co-extractions of multiple pesticide residues in vegetables[J]. Journal of Instrumental Analysis, 2008, 27(8): 795-799(in Chinese).
[11]	陈小华，汪群杰. 固相萃取技术与应用[M]. 北京：科学出版社，2010.
[12]	NY/T 1379—2007蔬菜中334种农药多残留的测定气相色谱质谱法和液相色谱质谱法[S]. 北京：农业出版社，2007.
[13]	GB 23200.8—2016水果和蔬菜中500种农药及相关化学品残留量的测定气相色谱-质谱法[S]. 北京：中国标准出版社，2017.
[14]	ANASTASSIADES M, LEHOTAY S J, STAJNBAHER D, SCHENCK F J. Fast easy multiresidue method employing acetonitrile extraction partitioning and ‘dispersive solid phase extraction’ for determination of pesticide residues in produce[J]. J AOAC Int, 2003, 86: 412-431.
[15]	BS EN 156622016 Foods of plant originmultimethod for the determination of pesticide residues using GC- and LC-based analysis following acetonitrile extraction/partitioning and cleanup by dispersive SPEModular QuEChERSmethod[S]. BSI Standards Publication, 2016.
[16]	BILLER J E, BIEMANN K. A novel approach for the utilization of gas chromatographmass spectrometer data[J]. Analytical Letters, 1974, 7(7): 515-528.
[17]	COLBY B N. Spectral deconvolution for overlapping GC/MS components[J]. J Am Soc Mass Spectrom, 1992(3): 558-562.
[18]	DROMEY R G, STEFIK M J, RINDFLEISCH T C, DUFFIELD A M. Extraction of mass spectra free of background and neighboring component contributions from gas chromatography/mass spectrometry data[J]. Anal Chem, 1976, 48(9): 1368-1375.
[19]	张伟国. 复杂基质（大米）中农药多残留分析方法研究[D]. 北京：中国农业大学，2006.
[20]	DAGAN S. Comparison of gas chromatographypulsed flame photometric detectionmass spectrometry, automated mass spectral deconvolution and identification system and gas chromatographytandem mass spectrometry as tools for trace level detection and identification[J]. Journal of Chromatography A, 2000, 868(2): 229-247.
[21]	NORLI H R, CHRISTIANSEN A, HOLEN B. Independent evaluation of a commercial deconvolution reporting software for gas chromatography mass spectrometry analysis of pesticide residues in fruits and vegetables[J]. Journal of Chromatography A, 2010, 1217(13): 2056-2064.
[22]	JOHNSEN L G, SKOU P B, KHAKIMOV B, BRO R. Gas chromatography mass spectrometry data processing made easy[J]. J Chromatogr A, 2017, 1503: 57-64.
[23]	DABROWSKI U. Evaluation of a simplified method for GC/MS qualitative analysis of polycyclic aromatic hydrocarbons polychlorinated biphenyls and organic pesticides using PARADISe computer program[J]. Molecules, 2020, 25(16): 3727-3736.
[24]	STAN H J. Application of capillary gas chromatography with mass selective detection to pesticide residue analysis[J]. Journal of Chromatography, 1989, 467(1): 85-98.
[25]	WEST S D, WESTON J H, DAY E W J. Gas chromatographic determination of residue levels of the herbicides trifluralin, benefin, ethalfluralin, and isopropalin in soil with confirmation by mass selective detection[J]. Association of Official Analytical Chemists, 1988, 71(6): 1082-1085.
[26]	李重九，费菁，刘建波. 色质联机多离子检测法（MID）用于黄瓜农药多残留分析的探讨[J]. 中国农业大学学报，1998,3(3):77-81. LI Chongjiu, FEI Qing, LIU Jianbo. Study on pesticides multiresidue analyses in cucumber by GC/MS (MID)[J]. Journal of China Agricultural University, 1998, 3(3): 77-81(in Chinese).
[27]	JULIE F, RALPH H, MARIO L, JENNIFER S. Multiresidue determination of pesticides in fruit and vegetables by gas chromatographymassselective detection and liquidchromatography with fluorescence detection[J]. Journal of AOAC International, 1995, 78(5): 1252-1266.
[28]	JULIE F, FRANCOIS S, JENNIFER S. Multiresidue method for the determination of residues of 251 pesticides in fruits and vegetables by gas chromatography/mass spectrometry and liquid chromatography with fluorescence detection[J]. Journal of AOAC International, 2000, 83(3): 698-713.
[29]	PANG G F, FAN C L, LIU Y M, CAO Y Z, ZHANG J J, LI X M, LI Z Y, WU Y P, GUO T T. Determination of residues of 446 pesticides in fruits and vegetables by threecartridge solidphase extractiongas chromatographmass spectrometry and liquid chromatographytandem mass spectrometry[J]. Journal of AOAC International, 2006, 89(3): 740-771.
[30]	ZWEIGENBAUM J. Mass spectrometry in food safety: methods and protocols[J]. Methods in Molecular Biology, 2011, 747: 199-201.
[31]	GB 23200.10—2016桑枝、金银花、枸杞子和荷叶中488种农药及相关化学品残留量的测定-气相色谱-质谱法[S]. 北京：中国标准出版社，2017.
[32]	GB/T GB 23200.9—2016粮谷中475种农药及相关化学品残留量的测定气相色谱-质谱法[S]. 北京：中国标准出版社，2017.
[33]	GB/T 23376—2009茶叶中农药多残留测定气相色谱/质谱法[S]. 北京：中国标准出版社，2010.
[34]	GB 23200.15—2016食用菌中503种农药及相关化学品残留量的测定气相色谱-质谱法[S]. 北京：中国标准出版社，2017.
[35]	GB/T 23744—2009饲料中36种农药多残留测定气相色谱-质谱法[S]. 北京：中国标准出版社，2009.
[36]	GB 23200.85—2016乳及乳制品中多种拟除虫菊酯农药残留量的测定气相色谱-质谱法[S]. 北京：中国标准出版社，2017.
[37]	GB 23200.7—2016蜂蜜、果汁和果酒中497种农药及相关化学品残留量的测定气相色谱-质谱法[S]. 北京：中国标准出版社，2017.
[38]	HJ 699—2014水质有机氯农药和氯苯类化合物的测定气相色谱质谱法[S]. 北京：中国环境科学出版社，2014.
[39]	HJ 743—2015土壤和沉积物多氯联苯的测定气相色谱-质谱法[S]. 北京：中国环境科学出版社，2015.
[40]	SHERIDAN R S, MEOLA J R. Analysis of pesticide residues in fruits, vegetables, and milk by gas chromatography/tandem mass spectrometry[J]. Journal of AOAC International, 1999, 82(4): 982-990.
[41]	WONG J W, ZHANG K, HAYWARD D G, KAIMENG C. Multiresidue pesticide analysis by capillary gas chromatographymass spectrometry[J]. Methods in Molecular Biology, 2011, 747: 131-172.
[42]	OKIHASHI M, TAKATORI S, KITAGAWA Y, TANAKA Y. Simultaneous analysis of 260 pesticide residues in agricultural products by gas chromatography/triple quadrupole mass spectrometry[J]. Journal of AOAC International, 2007, 90(4): 1165-1179.
[43]	ALDER L, GREULICH K, KEMPE G, VIETH B. Residue analysis of 500 high priority pesticides: better by GCMS or LCMS/MS?[J]. Mass Spectrometry Reviews, 2006, 25: 838-865.
[44]	MAESTRONIA B, BESILB N, BOJORGEC A, GREZC N, PREZPARADAC A, CANNAVANA A, HEINZENB H, CESIOB M W. Optimization and validation of a single method for the determination of pesticide residues in Peumus boldus Molina leaves using GC-MSD, GC-MS/MS and LC-MS/MS[J]. Journal of Applied Research on Medicinal and Aromatic Plants, 2020, 18: 100 254.
[45]	NGUYEN T D, YU J E, LEE D M, LEE G H. A multiresidue method for the determination of 107 pesticides in cabbage and radish using QuEChERS sample preparation method and gas chromatography mass spectrometry[J]. Food Chemistry, 2008, 110(1): 207-213.
[46]	SINHA S N, VASUDEV K, RAO M V V. Quantification of organophosphate insecticides and herbicides in vegetable samples using the "Quick Easy Cheap Effective Rugged and Safe" (QuEChERS) method and a highperformance liquid chromatographyelectrospray ionizationmass spectrometry (LC-MS/MS) technique[J]. Food Chemistry, 2012, 132: 1574-1584.
[47]	PIZZUTTI I R, KOK A D, ZANELLA R, ADAIMEA M B, HIEMSTRA M, WICKERT C, PRESTES O D. Method validation for the analysis of 169 pesticides in soya grain, without clean up, by liquid chromatography-tandem mass spectrometry using positive and negative electrospray ionization[J]. Journal of Chromatography A, 2007, 1142(2): 123-136.
[48]	PANG G F, CAO Y Z, FAN C L, JIA G Q, ZHANG J J, LI X M, LIU Y M, SHI Y Q, LI Z Y. Analysis method study on 839 pesticide and chemical contaminant multiresidues in animal muscles by gel permeation chromatography cleanup, GC/MS, and LC/MS/MS[J]. Journal of AOAC International, 2009, 92(3): s1-s72.
[49]	GB 23200.113—2018植物源性食品中208种农药及其代谢物残留量的测定气相色谱质谱联用法[S]. 北京：中国标准出版社，2018.
[50]	GB 23200.121—2021植物源性食品中331种农药及其代谢物残留量的测定液相色谱质谱联用法[S]. 北京：中国标准出版社，2021.

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Progress of Chromatography-Mass Spectrometry Technology and Development of Pesticide Multi-residue Analysis Methods (Part 2)——On the Selectivity of Low Resolution Mass Spectrometry

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