Advanced Search
LIANG Li-li, CHEN Jian, HOU Jing-li, ZHANG Li. Traces of Infant Formula Milk Powders by Elemental Analysis-Stable Isotope Ratio Mass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2015, 36(1): 66-71. DOI: 10.7538/zpxb.youxian.2014.0046
Citation: LIANG Li-li, CHEN Jian, HOU Jing-li, ZHANG Li. Traces of Infant Formula Milk Powders by Elemental Analysis-Stable Isotope Ratio Mass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2015, 36(1): 66-71. DOI: 10.7538/zpxb.youxian.2014.0046
shu

Traces of Infant Formula Milk Powders by Elemental Analysis-Stable Isotope Ratio Mass Spectrometry

  • 1.

    Instrumental Analysis Center, Shanghai Jiao Tong University, Shanghai 200240, China

  • 2.

    School of Pharmacy, Shanghai Jiao Tong University, Shanghai 200240, China

More Information
    Graphical Abstract
    • Abstract
  • In order to strengthen the supervision of the quality of infant formula milk powders which is the main food of infants，δ15N and δ13C of casein in infant formula milk powders were determined by elemental analysis-stable isotope ratio mass spectrometry(EA-IRMS). Casein which purity was over 96%， was extracted from milk powder by isoelectric-precipitation of proteins and identified by nano liquid chromatography & quadrupole-time-of-flight mass spectrometer(Nano LC-QTOF-MS). The ranges of δ15N and δ13C are correlated with the regional origins of infant formula powders. The values of δ15N and δ13C of casein from the milk powders with the same origin are very similar, whereas they are quite different with different origins. It is a reliable and convenient method to determine the regional origin of infant formula powders.
    • FullText(HTML)
    • References (21)
  • [1]
    高伟民. 婴幼儿配方奶粉发展现状及分析[J]. 饮料工业,2011,14(8):3-6.GAO Weimin. Status quo of and analysis on development of infant formula milk powder[J]. The Beverage Industry, 2011, 14(8): 3-6(in Chinese).
    [2]
    冯启. 聚焦当下中国婴幼儿奶粉的市场格局[J]. 乳品与人类,2012,(3):10-21.FENG Qi. Focus on the present market of infant milk powder in China[J]. Dairy and human, 2012, (3): 10-21（in Chinese）.
    [3]
    杨敦启. 奶粉掺杂物检测技术研究进展[J]. 中国乳业,2008,7(8):42-44.YANG Dunqi. Research progress in adulteration detection technology of milk powder[J]. China Dairy, 2008, 7(8): 42-44(in Chinese).
    [4]
    邓月娥,周群,孙素琴. 婴幼儿奶粉的FTIR分析与鉴定[J]. 光谱学与光谱分析,2006,26(4):636-639.DENG Yuee, ZHOU Qun, SUN Suqin. Analysis and discrimination of infant powdered milk via FTIR spectroscopy[J]. Spectroscopy and Spectral Analysis, 2006, 26(4): 636-639(in Chinese).
    [5]
    田志梅,张永顺. 紫外分光光度法快速测定液体奶、奶粉中蛋白质含量[J]. 中国卫生检验杂志,2008,18(2):263-264.TIAN Zhimei, ZHANG Yongshun. Rapid content determination of protein in liquid milk or milk power by UV spectrophotometry[J]. Cinese Journal of Health Laboratory Technology, 2008, 18(2): 263-264(in Chinese).
    [6]
    王定坤,冯志强,文灿,等. 全脂奶粉中蛋白质和氨基酸组成的比较[J]. 现代食品科技,2012,28(12):1803-1805.WANG Dingkun, FENG Zhiqiang, WEN Can,et al. Comparative studies of protein and amino acid composition in the whole milk powder[J]. Modern Food Science and Technology, 2012, 28(12): 1803-1805(in Chinese).
    [7]
    GB/T 50095—2010 食品中蛋白质的测定[S]. 北京：中国标准出版社，2010.
    [8]
    李宏梁,蕉茜楠,黄峻榕,等. 酪蛋白沉淀检测方法及其在牛乳经济掺假鉴定中的应用[J]. 食品科技,2008,33(12):262-266.LI Hongliang, JIAO Qiannan, HUANG Junrong, et al. Precipitation determination of casein and its application for economic adulteration identification in milk[J]. Food Science and Technology, 2008, 33(12): 262-267(in Chinese).
    [9]
    ROSSMANN A. Determination of stable isotope ratios in food analysis[J]. Food Reviews International, 2001, 17(3): 347-381.
    [10]
    郭波莉,魏益民,潘家荣. 同位素溯源技术在食品安全中的应用[J]. 核农学报,2006,20(2):148-153.GUO Boli, WEI Yimin, PAN Jiarong. Traceability technique of isotopic application in food satety[J]. Journal of Nuclear Agricultural Sciences, 2006, 20(2): 148-153(in Chinese).
    [11]
    钟石林. 稳定同位素技术在果汁中的应用[J]. 分析测试学报,2008,27(增刊1):221-223.ZHONG Shilin. Application of stable isotope ratio technique to fruit juices[J]. Journal of Instrumental Analysis, 2008, 27(Suppl 1): 221-223（in Chinese）.
    [12]
    薛洁,蒋露. SNIF-NMR和IRMS技术在原产地葡萄酒鉴定中的应用[J]. 食品与发酵工业,2011,37(10):154-158. XUE Jie, JIANG Lu. The preliminary research on wine geographical origins determination by SNIF-NMR and IRMS method[J]. Food and Fermentation Industries, 2011, 37(10): 154-158(in Chinese).
    [13]
    孙伟,张大明,汪聪慧. 海洛因来源鉴定的新方法[J]. 中国司法鉴定,2009,（3）:32-35.SUN Wei, ZHANG Daming, WANG Conghui. New methods of identifying illicit heroin origins[J]. Chinese Journal of Forensic Sciences, 2009, (3): 32-35(in Chinese).
    [14]
    郭波莉,魏益民,SIMON K D,等. 稳定性氢同位素分析在牛肉产地溯源中的应用[J]. 分析化学,2009,37(9):1333-1336.GUO Boli, WEI Yimin, SIMON K D, et al. Application of stable hydrogen isotope analysis in beef geographical origin traceability[J]. Chinese J Anal Chem, 2009, 37(9): 1333-1336(in Chinese).
    [15]
    SCAMPICCHIO M, MIMMO T, CAPICI C, et al. Identification of milk origin and process-induced changes in milk by stable isotope ratio mass spectrometry[J]. Journal of Agricultural and Food Chemistry, 2012, 60(45): 11268-11273.
    [16]
    李鑫,陈小珍,张东雷,等. 元素分析稳定同位素质谱同时测定δ13C/δ15N在原料乳粉检验中的应用[J]. 分析科学学报,2013,29(3):356-360.LI Xin, CHEN Xiaozhen, ZHANG Donglei, et al. Simultaneous detemination of δ13C and δ15N-in raw milk powder by elemental analysis isotope ratio mass spectrometry[J]. Journal of Analytical Science, 2013, 29(3): 356-360(in Chinese).
    [17]
    杨检林,李忠海,任国谱. 婴幼儿奶粉中含氮物质的研究进展[J]. 食品与机械,2008，24(1):164-168.YANG Jianlin, LI Zhonghai, REN Guopu. Review on nitrogenous substances in infant formula milk powder[J]. Food and Machinery, 2008，24(1): 164-168(in Chinese).
    [18]
    郭波莉,魏益民,潘家荣,等. 牛不同组织中稳定性碳同位素组成及变化规律研究[J]. 中国农业科学,2006,39(9):1885-1890.GUO Boli, WEI Yimin, PAN Jiarong, et al. Study on the change of stable carbon isotope composition in cattle tissues[J]. Scientia Agricultura Sinica, 2006, 39(9): 1885-1890(in Chinese).
    [19]
    PIASENTIERA E, VALUSSOA R, CAMIN F, et al. Stable isotope ratio analysis for authentication of lamb meat[J]. Meat Science, 2003, 64(3): 239-247.
    [20]
    祁茹,林英庭. 同位素溯源技术在动物产品和饲料成分溯源中的应用[J]. 中国奶牛,2010,(5):45-48.QI Ru, LIN Yingting. Application of isotope tracer techniquein animal product and feed ingredients[J]. China Dairy Cattle, 2010, (5): 45-48（in Chinese）.
    [21]
    张乃武,梁明,宋伟新. 从奶粉中分离酪蛋白、乳糖、乳脂的研究[J]. 牡丹江师范学院学报：自然科学版,2004,(1):30-31.ZHANG Naiwu, LIANG Ming, SONG Weixin. Research in separation of casein, lactose and milk fat from milk powder[J]. Journal of Mudanjing Teachers College(Natural Sciences Edition), 2004, (1): 30-31(in Chinese).
    • Related Articles

  • Related Articles

    [1]ZHANG Han-yu, JIE Zhao-wei, ZHENG Han-yang, ZHU Xiao-han, XIE Wei-ya, HU Can, LIU Zhan-fang, GUO Hong-ling, ZHU Jun, MEI Hong-cheng. Examination and Tracing of Stable Isotopes of Carbon and Hydrogen in Diesel Oil from Different Regions[J]. Journal of Chinese Mass Spectrometry Society, 2025, 46(2): 196-205. DOI: 10.7538/zpxb.2024.0068
    [2]YIN Xi-jie, LIU Wei-wei, WANG Yong-tao, SU Jing, LI Ting-wei. Determination of δ15N on Microgram Amounts by Modified Element Analysis-Isotope Ratio Mass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2021, 42(3): 346-352. DOI: 10.7538/zpxb.2020.0051
    [3]LIU Chang-jing, MEI Hong-cheng, ZHU Jun, HE Ya, HE Xin-long, JIANG Jing, QUAN Yang-ke, WANG Gui-qiang. Selection of Reference Materials for Hydrogen Stable Isotope Detection of Human Hair[J]. Journal of Chinese Mass Spectrometry Society, 2019, 40(4): 342-348. DOI: 10.7538/zpxb.2018.0144
    [4]MENG Xian-jing, YANG Bin, MA Xiao, ZHANG Hong-bo, XU Bo, WANG Xu, YIN Song. Application of Temperature-Ramped GC on δ15N, δ13C and δ34S Measurements Using EA-IRMS System[J]. Journal of Chinese Mass Spectrometry Society, 2018, 39(5): 630-639. DOI: 10.7538/zpxb.2018.0025
    [5]DAI Qi, ZHONG Qi-ding, WANG Dao-bing, WU Zhu-ying, CHEN Shan-shan, XIAO Dong-guang. Study on Stable Carbon and Nitrogen Isotope Characteristics of Cage-Free Eggs and Caged Eggs[J]. Journal of Chinese Mass Spectrometry Society, 2016, 37(4): 366-373. DOI: 10.7538/zpxb.2016.37.04.0366
    [6]TAN Meng-ru, LIN Hong, SHEN Chong-yu, WU Bin, ZHANG Rui, DING Tao, FEI Xiao-qing, YANG Gong-jun. Detection of Fermented Soy Sauce Adulteration Using Elemental Analyzer-Carbon Isotope Ratio Mass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2015, 36(4): 334-340. DOI: 10.7538/zpxb.youxian.2015.0016
    [7]WANG Lei, ZHONG Qi-ding, WANG Dao-bing, LIU Ming, TAO Hong-bing, WU Zhu-ying, XIONG Zheng-he, XIAO Dong-guang. The Impact of Forage on the Stable Carbon Isotope Composition in Milk[J]. Journal of Chinese Mass Spectrometry Society, 2014, 35(4): 378-384. DOI: 10.7538/zpxb.2014.35.04.0378
    [8]FEI Xiao-qing, SHEN Chong-yu, WU Bin, ZHANG Rui, DING Tao, ZHANG Xiao-yan, CHEN Lei. Detection of Royal Jelly Adulteration Using Elemental Analyzer-Carbon Isotope Ratio Mass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2014, 35(2): 144-148. DOI: 10.7538/zpxb.2014.35.02.0144
    [9]CUI Jie-hua, QI Biao, WANG Yan-hong. Measurement of Stable Carbon Isotopic Composition of Plant Samples by EA-IRMS System[J]. Journal of Chinese Mass Spectrometry Society, 2008, 29(1): 24-29.
    [10]WANG Xu, ZHANG Fu-song, DING Zhong-li. Changes in the Combustion Transformation Capability of EA-Conflo-IRMS and Their Impacts on Nitrogen and Carbon Isotope Ratio Measurement[J]. Journal of Chinese Mass Spectrometry Society, 2006, 27(2): 104-109.

Catalog

    Get Citation
    PDF
    XML
    Article views (864) PDF downloads (991) Cited by()
    Turn off MathJax
    Article Contents
    Abstract
    References
    Related Articles
    Links

    Website Copyright © 2023 Journal of Chinese Mass Spectrometry Society  京ICP备12043220号-2

    Address: Box 65, P.O. Box 275, Beijing    Postal Code: 102413     Tel:010-69357734     E-mail:jcmss401@163.com

    Supported by: Beijing Renhe Information Technology Co., Ltd.  Baidu Analytics

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return