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ZHANG Jing-bo, DONG Zhen-lin, ZHAO Shou-cheng, JIANG Wen-feng, WEI Feng. Simultaneous Determination of Triazine Herbicides in Maize by Gas ChromatographyMass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2006, 27(3): 148-154.
Citation: ZHANG Jing-bo, DONG Zhen-lin, ZHAO Shou-cheng, JIANG Wen-feng, WEI Feng. Simultaneous Determination of Triazine Herbicides in Maize by Gas ChromatographyMass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2006, 27(3): 148-154.
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Simultaneous Determination of Triazine Herbicides in Maize by Gas ChromatographyMass Spectrometry

  • 1.

    Dalian University of Technology, Dalian 116024, China

  • 2.

    Technology Centre, Liaoning Entry-Exit Inspection and Quarantine Bureau, Dalian 116001, China

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  • Corresponding author:

    WEI Feng

  • Received Date: January 19, 2006
  • Revised Date: April 17, 2006
    Graphical Abstract
    • Abstract
  • A multi-residue method for determination of 21 kinds of triazine herbicides in maize was described. The triazine herbicide residues were extracted with acetonitrile and cleaned up with strong cation-exchange solid-phase extraction column. The extraction was separated by capillary column (DB-5MS, 30 m×0.25 mm ×0.25 μm) and detected by GC/MS. The good linearities were obtained for 21 triazine herbicides. The limits of quantitation were 0.01mg/kg. The average spiked recoveries ranged from 84.0% to 104.1% and the relative standard deviations were between 0.8% and 5.1%.
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    • References (8)
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