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WANG Jian, PAN Yang. Photoionization Mass Spectrometric Study on Several Aldehydes and Ketones in Cigarette Mainstream Smoke[J]. Journal of Chinese Mass Spectrometry Society, 2012, 33(5): 265-270.
Citation: WANG Jian, PAN Yang. Photoionization Mass Spectrometric Study on Several Aldehydes and Ketones in Cigarette Mainstream Smoke[J]. Journal of Chinese Mass Spectrometry Society, 2012, 33(5): 265-270.
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Photoionization Mass Spectrometric Study on Several Aldehydes and Ketones in Cigarette Mainstream Smoke

  • 1.

    Technology Center of Shanghai Tobacco Group Corporation, Shanghai 200082, China

  • 2.

    National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230029, China

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  • Received Date: December 31, 1899
  • Revised Date: December 31, 1899
    Graphical Abstract
    • Abstract
  • Formaldehyde, ketene, acetaldehyde, propanal and acetone in the gas phase of cigarette mainstream smoke were studied by synchrotron photoionization/time-of-flight mass spectrometry (TOF-MS). The mass-to-charge ratios (m/z) of these aldehydes and ketones can be obtained from photoionization mass spectra at different photon energies. Moreover, by tuning photon energies, the photoionization efficiency (PIE) curves of these compounds can be measured. Hence, structural identification can be fulfilled by comparing the measured PIE curves and ionization energies (IEs) with standard photoionization cross sections and IEs.
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    • References (20)
  • [1]
    BAKER R R. Smoke chemistry in tobacco: Production, chemistry and technology (Davis, L.D., and Nielsen, M.T., Eds.)[J]. Blackwell Science, Oxford, U.K, 1999: 398-439.
    [2]
    WAKEHAM H. Recent trends in tobacco and tobacco smoke research. In Proceedings of the symposium on the chemical composition of tobacco and tobacco smoke (Schmeltz, I., Ed.) [J]. 162nd National Meeting of the American Chemical Society, Washington, DC: 1-20.
    [3]
    World health organization geneva. Enviromental health criteria 89 [R]. 1989.
    [4]
    徐济仓, 侯英, 杨式华, 等. 高效液相色谱法测定卷烟主流烟气中的低分子醛酮类化合物 [J]. 环境化学, 2006, 25 (6): 678-682.
    [5]
    黄云, 王裔耿, 缪明明, 等. 快速分离柱高效液相色谱法测定卷烟主流烟气中的主要羰基化合物[J]. 色谱, 2007, 25 (2): 230-233.
    [6]
    WANG J, WEN J J, JIA L Y, et al. Study on gas phase components in mainstream cigarette smoke by synchrotron radiation photoionization mass spectrometry [J]. Chin J Anal Chem, 2012, 40 (7): 1048-1052.
    [7]
    ESCHNER M S, SELMANI I, GROGER T M, et al. Online comprehensive two-dimensional characterization of puff-by-puff resolved cigarette smoke by hyphenation of fast gas chromatography to single-photon ionization time-of-flight mass spectrometry: Quantification of hazardous vcolatile organic compounds [J]. Anal Chem, 2011, 83 (17): 6 619-6 627.
    [8]
    MITSCHKE S, ADAM T, STREIBEL T, et al. Application of time-of-flight mass spectrometry with laserbased photoionization methods for time-resolved on-line Analysis of Mainstream Cigarette Smoke [J]. Anal Chem, 2005, 77 (8): 2 288-2 296.
    [9]
    MUHLBERGER F, STREIBEL T, WIESER J, et al. Single photon ionization time-of-flight mass spectrometry with a pulsed electron beam pumped excimer VUV lamp for on-line gas analysis: Setup and first results on cigarette smoke and human breath [J]. Anal Chem, 2005, 77 (22): 7 408-7 414.
    [10]
    ADAM T, MITSCHKE S, STREIBEL T, et al. Puff-by-puff resolved characterization of cigarette mainstream smoke by single photon ionization (SPI) time-of-flight mass spectrometry (TOFMS): Comparison of the 2R4F research cigarette and pure Burley, Virginia, Oriental and Maryland tobacco cigarettes [J]. Anal Chim Acta, 2006, 572 (2): 219-229.
    [11]
    YANG B, OβWALD P, LI Y Y, et al. Identification of combustion intermediates in isomeric fuel-rich premixed butanol-oxygen flames at low pressure [J]. Combust Flame, 2007, 148 (4): 198-209.
    [12]
    齐飞. 燃烧：一个不息的话题——同步辐射单光子电离技术在燃烧研究中的应用[J]. 物理, 2006, 35 (1): 1-6.
    [13]
    TAATJES C A, HANSEN N, MCLLROY A, et al. Enols are common intermediates in hydrocarbon oxidation [J]. Science, 2005, 308 (5 730): 1 887-1 889.
    [14]
    PAN Y, ZHANG T, HONG X, et al. Fragment-controllable mass spectrometric analysis of organic compounds with an infrared laser desorption/tunable vacuum ultraviolet photoionization technique [J]. Rapid Commun Mass Spectrom, 2008, 22 (10): 1 619-1 623.
    [15]
    PAN Y, YIN H, ZHANG T C, et al. The characterization of selected drugs with IR laser desorption/ tunable synchrotron VUV photoionization mass spectrometry [J]. Rapid Commun. Mass Spectrom, 2008, 22 (16): 2 515-2 520.
    [16]
    HUANG C, YANG B, YANG R, et al. Modification of photoionization mass spectrometer with synchrotron radiation as ionization source [J]. Rev Sci Instrum, 2005, 76 (12): 126108.
    [17]
    LINSTROM P J, MALLARD W J. NIST Chemistry Webbook, National Institute of Standard and Technology, Number 69, Gaithersburg, MD, 2005, http://webbook.nist.gov.
    [18]
    金平正，金闻博. 卷烟烟气安全性与危害防范[M]. 北京：中国轻工业出版社, 2009.
    [19]
    KANG J C, CHEN P H, JOHNSON W R. Ketene formation in pyrolysis of carbohydrates[J]. Abs Pap Am Chem Soc, 1976, 172 (3): 106.
    [20]
    KANG J C, CHEN P H, JOHNSON W R. Ketene formation from the pyrolysis of carbonhydrates. Thermal uses and properties of carbohydrates and lignins[J]. Edited by F Shafizadeh, New York: Academic Press, 1976: 261-273.
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