微区原位元素及同位素分析标准物质研究进展
Recent Progress of Reference Materials for In-situ Elemental and Isotopic Microanalysis
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摘要: 微区原位分析技术具有简单、快速、实时在线、空间分辨率高等优点，近年来广泛应用于地球科学、材料科学、生命科学等领域。微区原位分析时，样品前处理过程的省略不可避免地产生显著的基体效应，制约着微区原位分析结果的准确性和可靠性。在测量中使用微区分析标准物质，尤其是与待测样品基体匹配的标准物质对结果进行校正，是克服基体效应最直接有效的方法，是获得可靠测量结果的必要保障。目前，相关微区分析计量标准严重匮乏，导致微区原位测量结果的准确性和可靠性难以保证，这已成为制约其进一步应用和发展的瓶颈，也是相关应用领域和计量研究机构关注的热点。本文系统介绍了微区原位元素及同位素分析用标准物质，包括微区标准物质的技术要求、制备技术、标准样品和标准物质现状等，并对微区原位分析标准物质的发展趋势进行展望。Abstract: In-situ microanalysis technology has been extensively used in the fields of geoscience, material analysis and bioimaging due to its advantages including simplicity, rapidity, real-time online, spatial resolution, etc. However, without proper sample pretreatment and separation process, the complex sample matrix will have a significant impact on the measured results, i.e. matrix effect, which should be properly corrected by using the matrix-matched reference material. Meanwhile, due to the grave shortage of related reference material, the traceability of in-situ microanalysis has not been properly solved, it is difficult to obtain comparable and reliable measurements. This situation has become a bottleneck that hinders the application and development of in situ microanalysis technology, and is also the focus of relevant application fields and institutes of metrology. In this review, the reference materials for in situ elemental and isotopic microanalysis were systematically introduced, including technical requirements, preparation technology and existing reference materials, etc. Furthermore, the development tendency of reference materials for in situ microanalysis was prospected.
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