用GC/MS测定大葱挥发油中的化学成分

  • 摘要: 本工作采用水蒸汽蒸馏法,分别从大葱的葱白、葱叶、葱花中提取挥发油,用毛细管气相色谱-质谱法定性鉴别了挥发油中的18种化学成分。主要成分有:二甲基二硫醚、二甲基三硫醚、甲基丙基二硫醚、甲基丙基三硫醚、甲基丙烯基二硫醚、甲基丙烯基三硫醚、丙基丙烯基二硫醚、丙基丙烯基三硫醚、二丙基三硫醚等含硫化合物,以及2-甲基-2戊烯醛、2-十三酮等含氧化合物。文中还比较了大葱挥发油和洋葱挥发油中化学成分的相对含量。

     

    Abstract: Study on the Chemical Constituents of Volatile oil in Green Chinese Onions(Allium Fistulosum L)Guo Haichen;Gui Lan;Zhu Qianxiang;Zhou Xiuqing;Wang Ling(Analytical and Testing Center,Jilin University Changchun 130023,China)Received Abstract:Three volatile oils were individually obtained from distillation of stem,leaf and flower of green Chinese onions(Allium fistulosum L).18 chemical constituents in volatile oils were identified with capillary gas chromatography-mass spectrometry.Main components are sulfur-containing compounds such as dimethyl disulfide,dimethyl trisulfide,methyl propyl disulfide,methyl propyl trisulfide,methyl propenyl disulfide,methyl propenyl trisulfide,propyl propenyl diSulfide,propyl propenyl trisulfide,dipropyl trisulfide etc as well as oxygen-containing compounds such as 2-methyl-2-pentenal,2-tridecanone etc.In the paper,the relative content comparison of chemical constituent between green Chinese onions oil and onion oil was given too.Keywords:Allium fistulosum L; volatile oil,GC/MS

     

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